TBfinalprojectmodified1.docx

COLLEGE OF ENGINEERING

DEPARTMENT OF MECHANICAL & INDUSTRIAL ENGINEERING

BEng (Honours) in Computer Aided Mechanical Engineering

Academic Year: 2018-19 Semester: B

MHH124725: Technical Project

Final Report

Project Title: Corrosion Analysis of Aluminum Alloy 7075.

Student Name: Amani Al Ajmi

Student Number: 140150

Supervisor(s): Mr. Said Al Oraimi

Declaration by the Student

I declare that this project report / dissertation titled _____________________________

________________________________________________________________________

is my own work and has not been submitted in any form for another degree or diploma at any university or other institutions of tertiary education. Information derived from the published work of others has been acknowledged in the text and a list of references is given. I am fully aware of the College’s policy on plagiarism and cheating, and that the penalty for submission of plagiarized report could result in a ‘fail’ in Technical Project / Dissertation. I have submitted a copy of this full report in electronic form to my supervisor.

Signature of the Student: Date:

Name of the Student:

Student Number:

Certificate by the Supervisor

The project report / dissertation titled _________________________________________

_______________________________________________________________________

is the bonafide work of Mr./ Ms. ______________________________________________, and bearing student number ______________ is carried out under my supervision. I certify that the work presented in the project report / dissertation is carried out by him / her, and that he / she has achieved the set objectives of the project / dissertation. Information derived from the published work of others has been acknowledged in the text and a list of references is given at the end of the report. I have personally checked this final report for originality / plagiarism through the Turnitin website and, to the best of my knowledge and belief, satisfied that the report is free from plagiarism.

Signature of the Supervisor: Date:

Name of the Supervisor:

Countersigned by HoD:

ACKNOWLEDGEMENT

The acknowledgement by the candidate for successfully carrying out the project work

ABSTRACT

Aluminum plays an important role in a number of industrial applications such as construction and electrical engineering. It is also quite applicable in the transport industry where it is used in the manufacturing and production of machinery used in the aircraft building. Although aluminum and its alloys are quite useful, they are subject to corrosion as a result of chemical interaction with the surroundings and hence do not the best materials for engineering applications. One of the main significant problems faced by aluminum components used in the aircraft is pitting corrosion. An experimental analysis of components of aluminum in aircraft to identify corrosion will be carried out in this project. Findings indicate severe corrosion of nose landing component leading to its failure. Pitting corrosion refers to the restricted high metal dissolution as a result of depletion of the passive film on the metal surface that acts as a protective cover. This study aims at bringing into discussion an analysis of corrosion in the aluminum alloy (7076) mainly used in aircraft components. Therefore, this project identifies the details on materials, undertaking taste samples on the identified materials, and measures are undertaken to improve corrosion resistance. Hence, development of the two types of coating, and testing their levels of resistance to corrosion.

This experiment identifies two types of heat treatment experiments useful in testing samples with and without coating condition. An examination will be carried out on the behavior of the metal using hardness testing before and after heat treatment, measurement of the surface roughness, corrosion test in sea water followed with an acid test. Analysis of these results finally will be carried out to achieve the objectives successfully.

 

‏Keywords: Aluminum alloy (7076)، Pitting corrosion, Hardness testing, Heat treatment.

TABLE OF CONTENTS

The content shall follow the abstract and indicate the page numbers of the chapters, sections, sub-sections, appendices and references. The number and titles of all the items must be clearly entered with page numbers against them.

LIST OF TABLES

Table Number

Description

Page No.

Table 4.1

Hardness readings before heat treatment.

Table 4.2

Hardness readings after heat treatment.

Table 4.3

Roughness measurements.

Table 4.4

Weight loss.

LIST OF FIGURES

Figure Number

Description

Page No.

Figure 1.1

Pitting Corrosion.

Figure 1.2

Aircraft Material.

Figure 3.1

Morgen Rushworth RGMS.

Figure 3.2

Aluminum Alloy Sheet Before cutting.

Figure 3.3

Aluminum Alloy Sample After cutting.

Figure 3.4

Metallic Stamp.

Figure 3.5

Hammer.

Figure 3.6

Samples After Numbering.

Figure 3.7

Aluminum Oxide and Aluminum paint.

Figure 3.8

During the Painting Step.

Figure 3.9

Sample After Applying the First layer of Coating.

Figure 3.10

Zinc Spray and the Samples Before Coating.

Figure 3.11

The Samples After Zinc Coating.

Figure 3.12

Underbody Rubber Spray.

Figure 3.13

The Samples After Rubber Coating.

Figure 3.14

Furnace during

Figure 3.15

Quenching Samples in Water.

Figure 3.16

Rockwell Hardness.

Figure 3.17

Indenter Used for Testing.

Figure 3.18

Roughness Device (Mitutoyo) connected to Computer Software.

Figure 3.19

During Roughness Measurement for Zinc Sample.

Figure 3.20

Samples immersed in Seawater.

Figure 3.21

Apparatus used for HCL Test.

Figure 3.22

HCl Solution.

Figure 3.23

Sample Without Coating Initial Weight.

Figure 3.24

Sample Without Coating Weight After Seawater and HCL Tests.

Figure 3.25

Zinc Sample Initial Weight.

Figure 3.26

Zinc Sample Weight After Seawater and HCL Tests.

Figure 4.1

Hardness Readings Before Heat Treatment.

Figure 4.2

Hardness Readings After Heat Treatment.

Figure 4.3

Zinc Sample Roughness Profile.

Figure 4.4

Underbody Rubber Sample Roughness Profile.

Figure 4.5

Aluminum Oxide Sample Roughness Profile.

Figure 4.6

Without Coating Sample Roughness Profile.

Figure 4.7

Rz and Rq Values of the Samples.

Figure 4.8

Weight Loss (g) of the Samples.

LIST OF SYMBOLS AND ABBREVIATIONS

NaCl – Sodium Chloride.

HCL – Hydrochloric Acid.

H2O – Water.

Al – Aluminum.

% – Percentage.

Zn – Zinc.

Al2O3 – Aluminum Oxide.

PH – Potential Hydrogen.

Chapter name & title

1

16

CHAPTER 1 INTRODUCTION

1. Introduction.

Corrosion is the deterioration of materials by chemical interaction with the surrounding environment; it is a natural phenomenon which can be controlled by correcting the condition when an early warning signs occurs. Airframe issues related to corrosion have plagued the aerospace industry for decades. The metals of aircraft components are exposed to different forms of corrosion; there are many agents which accelerates the corrosion process such as prolonged exposure to corrosive factors including moisture, salts and industrial fluids. The main source of corrosion is water vapor containing salt that combines with the oxygen in the air. The appearance of corrosion differs depending on the type of the metal, on the aluminum alloy surface it shows as pitting which is combined with white or gray powdery deposit. This project will provide an experimental study on the corrosion analysis of aluminum alloy where 75% of aircraft structures are made of aluminum as shown in Figure 2.

Figure 1.1 Pitting Corrosion

Figure 1.2 Aircraft material

1.1 Problem statement:

Pitting corrosion is one of the most common problems faced by aluminum components used in aircraft, as the name implies this type of corrosion means the formation of small holes in the surface of the material. Due to the high-speed landing of aircraft on the dusty runway, the protective coating is removed which lead to the exposure of the metals surface to the corrosive factors.

1.2 The aim of the project:

To perform an experimental study about corrosion analysis of aluminum alloy material used in aircraft component.

1.3 The main objectives:

· Identify the causes of corrosion.

· Carry out the corrosion resistance process experimentally.

· Analyze the obtained result.

1.4 Scope of studies:

· Literature review about corrosion in aluminum alloy material.

· Investigate and understand the working principle of the metal coating and heat treatment to reduce the corrosion in aluminum alloy.

· Implement roughness measurement of the coated samples followed by corrosion test with sea water and acid.

1.5 Importance of the research:

Understanding and analyzing the corrosion behavior is important, there are many factors regarding the significance of corrosion study including economic, by implement corrosion control process, the useful life of aircraft can be extended, therefore the maintenance cost will be reduced. Also, the best insurance against corrosion associated failures is studying and testing the metals used in the design of the planes in order to select the proper ways to control the problem to increase the safety of public.

CHAPTER SUMMARY

Corrosion is considered to be a natural phenomenon which can be controlled through changing or altering the conditions immediately after early warning signs are detected. Corrosion has been a major concern within the Aerospace industry where it has been leading to issues related to Airframe. In Aerospace industry, metals of aircraft are becoming exposed to corrosion and this activity is accelerated by prolonged exposure to corrosive agents like moisture, salts, and industrial fluids. Water vapor is considered to be the primary source of corrosion and it is composed of salts which combine with oxygen in air.

One of the metals affected as a result of pitting corrosion is aluminum components used in aircraft leading to the formation of small holes in the surface of the material. This study aims at identifying the causes of corrosion; carrying out the corrosion resistance process experimentally; and analyzing the obtained result. The scope of this study is to investigate and understand the working principle of the metal coating and heat treatment to reduce the corrosion in aluminum alloy; and implement roughness measurement of the coated samples followed by corrosion test with sea water and acid. There are a number of advantages associated with this study. Through implementation of corrosion control process, it is possible to extend the life of aircraft can be extended thus helping in reducing the maintenance cost.

CHAPTER 2: LITERATURE REVIEW

2. Introduction.

Corrosion refers to the process of material degradation as a result of interaction with the environment. Corrosion occurs in metals, polymers, and ceramics. The research on corrosion and its alloys is an enormous area of research since it involves a broad range of applications in areas such as marine, aerospace, industrial and family environments. The main reason for its usage is due to the good machinability, weldability, and good corrosion resistance. Corrosion resistance of alloys is attributed to the fact that they are naturally developing to an oxide film on their surface as a result of environmental condition. However, pitting corrosion is the main corrosion phenomenon which is common and occurring due to the breakage in the oxide film.

Resistance to pitting of the metals is influenced by the physical, electrical, and mechanical features of the passive layer. As a result of perfect passivity with greater uniform corrosion resistance to seawater, pitting remains the primary concern for Aluminium Alloys in the environment with seawater.

This chapter includes some literature reviews which have been referred to regarding corrosion analysis of Aluminum alloy.

2.1 Effect of heat treatment on some mechanical properties of 7075 aluminium alloy.

Adeyemi Dayo Isadare, Bolaji Aremo, Mosobalaje Oyebamiji Adeoye, Oluyemi John Olawale, Moshood Dehinde Shittu, (2013) work entails a detailed explanation of their experiment which involved an examination of annealing on micro-structural morphology as well as mechanical properties of 7075 Al alloy. Additionally, the experiment evaluated the relationship between age hardening on microstructural characteristics of 7075 alloy. The researchers concluded from the experiment results that annealing heat treatment had the power to do away with micro-segregation. Age hardening heat treatment was also observed to bring an improvement on mechanical characteristics of the Alloy (Isadare, Aremo, Adeoye, Olawale & Shittu, 2013). This work perfectly fits the topic since it shed light on how the project topic can be handled. This stem from the fact that the work reveals that age hardening heat treatment can improve the mechanical property of the aluminum alloy. One such characteristic is resistance to corrosion. To make the allow resistant to corrosion by other elements or acids using the results from Adeyemi Dayo Isadare, Bolaji Aremo, Mosobalaje Oyebamiji Adeoye, Oluyemi John Olawale, Moshood Dehinde Shittu (2013) work it’s hence recommendable to do age hardening heat treatment.

2.2 Quenching of aluminum alloys: cooling rate, strength, and inter-granular corrosion‖.

Patricia Kavalco, Canale Lauralice and George Totten (2009) research entails the study of intergranular corrosion. The researchers investigated how intergranular corrosion could be used to reduce corrosion. In the study, it was found out that the cooling rate of any aluminum alloy determined the rate of pitting corrosion. The slower the rate of cooling the fewer chances an aluminum allow being affected by corrosion. On the other hand, if an alloy was quickly cooled the impact would be that the alloy would be easily corroded by corrosive reagents or chemicals (Kavalco, Lauralice & Totten, 2009). On that note, the authors recommend that while making any aluminum allow it was crucial to give attention to the cooling rate. In the event that the alloy will be exposed to highly corrosive agents, it is advisable to have the cooling rate very slow and vice versa. This work is useful in informing the topic that is corrosion in Aluminum alloy. With the findings from the source, one can state that corrosion in aluminum alloys is dependent on the rate of cooling of the alloy during its making.

2.3 Improvement Properties of 7075-T6 Aluminum Alloy by Quenching in 30% Polyethylene Glycol and Addition 0.1%B‖.

Jasim Salman, Shaymaa Alsada and Khadim Al-Sultani (2013) work discusses the results of their experiment. The experiment was set up to investigate the impact of sodium chloride, polyethylene glycol and boron on aluminum alloy. The authors wanted to know whether the combination of these solutions or elements could improve the feature of the 7075-T6 alloy. The target features were corrosion resistance, toughness as well as thermal aging behavior. The researchers took 3.5% NaCl, 30% polyethylene glycol and Boron solution and treated 7075- T6 alloy with. The results indicated that the solution improved the toughness feature of the alloy by 50%. However, the corrosion property was not significantly influenced by the solution. This indicates that the solution cannot be used to improve the corrosion resistance of the alloy (Salman, Alsada& Al-Sultani, 2013). Generalizing the case to other types of aluminum alloys one can draw an insight that a mixture of boron, sodium chloride and polyethylene glycol have no properties in improving the corrosive resistance feature of an aluminum alloy. On that note, the work is significant in this topic since it gives direction on elements and solution which should not be used while improving the resistance features of an aluminum alloy.

2.4 Recent developments in advanced aircraft aluminum alloys.

Tolga Dursun and Costas Soutis (2014) work is about their review on the recent aluminum technology employed in aircraft industry which is one area aluminum alloys are industrially exploited. The authors learned that the technology has led to having damage tolerant, strong, tough and corrosion resistant alloys. The review shows that a combination of Aluminum and zinc leads to a very strong alloy. Mixing Aluminum and copper results to a high damage resistant alloy. Of key importance in this context is mixing aluminum and lithium that is AL-Li. The outcome is an alloy with improved properties such that the alloy is has higher fracture toughness and is corrosion resistant (Dursun& Soutis, 2014). This work is essential in the study of this topic from the angle that it shows the right chemical composition that can be used to have a high corrosion resistant alloy.

2.5 Aluminum Alloys for Aerospace Applications‖, Aerospace Materials, and Material Technologies.

The work entails a history of aerospace technology with aluminum alloys in focus. Also, entails classification of aluminum alloys. The classification is based on temperatures used to heat and cool the alloys. This is because the temperatures are a significant determinant of the strength property as well as other features (Rambabu, Prasad& Wanhill, 2017). Additionally, the work entails weaknesses or gaps in the current aluminum technology used in aerospace. These gaps are crucial in handling the topic given that they will show areas that require more research in improving the corrosion resistance feature of aluminum alloys.

2.6 Aluminium alloy corrosion of aircraft structures: modelling and simulation.

To prevent corrosion occurrences, Aluminum and its alloys were properly handled using various protection methods that prevent corrosion of the aircraft. These methods include: waxing, painting, zinc-chromate priming, coating using thin layer of Alclad, anodizing and coating with a liquid protective solution (DeRose, 2013 pg. 23-29).

Barrier coating using materials such as paint, plastic, wax or powder was applied and left out for some time for later observations. Aluminum was also coated using a thin layer of pure aluminum. Pure aluminum was successfully sprayed on the aluminum flat and round coupons at low temperatures. Hardness test was then carried out before and after the heat treatment Demo, (Steiner, Friedersdorf, and Putic, 2010 pg. 1-9). Aluminum specimen was heated at 500 Celsius and then quenched in cold oil. Hardness of the heat-treated specimen and those without heat treated specimen was measured in and recorded. Resistance to corrosion of the samples was evaluated in 3.5 % sodium chloride solution by weight loss method. Corrosion test was also conducted in wet conditions which included seawater and hydrochloric water conditions. Roughness measurements were also conducted on the final product.

2.7 Milestone case histories in aircraft structural integrity.

We found out that epoxy, nylon and urethane which are types of powders, which were heated and placed on the aluminum surface to form a thin film layer offered protection from corrosion. Plastic and waxes which were sprayed onto the aluminum surfaces acted as a coating to offer protection to aluminum surface from mixing with other corrosive elements that lead to corrosion (Wanhill, Molent, Barter and Amsterdam, 2015 pg. 346) People have come up with current painting systems in the aircraft components that combine different painting layers which have been designed to serve different functions. They are usually applied in three layers. The first spray paint acts as the inhibitor which decreases the activity of the aluminum and its alloys or blocks it from combining or reacting with other corrosive elements. The second and intermediate layers of paint coats are applied to add to the overall thickness of the paint and to make sure that no aluminum surface is left exposed (Kiyak, 2012 pg. 9-16) The last and finish coat is primarily designed to offer resistance to the environmental factors such as humidity, pH concentration and alkaline concentration of the surrounding. We also found out that pure aluminum coating component insulates and protects aluminum from corroding. This helped in reducing the extent of corrosion.

2.8 Can pitting corrosion change the location of fatigue failures in aircraft?

Regarding hardness test, it was found out that after heat treatment at 500 °C and subsequent quenching in oil of aluminum component the hardness and corrosion resistance of pure aluminum improved whereas before heat treatment, the hardness and corrosion resistance of the material was low. Concerning corrosion in wet areas, we found out that aluminum corrodes faster or quicker when placed in wet areas. This is because the water component acts as a catalyst in the process of corrosion (Crawford, Loader, Liu, Harrison, and Sharp, 2014 pg. 304-314). When Aluminum, which is the material used to make aircrafts, is left unprotected in certain areas such as salty areas near the ocean or sea waters, it will form an oxide layer and corrodes almost immediately. Because of the corrosive action of this strongest of acids like hydrochloric acid on metals like aluminum, normally, non-metal materials are preferred, when possible (Jaya, Tiong, and Clark, 2012 pg. 64-73). Aluminum have useful corrosion resistance in low concentrations of HCl. The corrosivity increases dramatically as the concentration of HCl and temperature increase. This led to an increased rate and extent of corrosion. Therefore, the extent of destruction was higher in wet areas as compared to that one in dry areas.

2.9 Recent developments in advanced aircraft aluminium alloys. Materials & Design.

The main disadvantage of using coating as a method of preventing corrosion is that the coating components need to be reapplied over and over again which is tiring and expensive. Poorly applied coatings always fail and can lead to increased rate and increased extent of corrosion (Dursun and Soutis, 2014 pg. 862-871). Sometimes, there might exist some volatile organic components in certain coatings which make them vulnerable to corrosion.

2.10 Role of chemical composition in corrosion of Aluminum Alloy.

The current political environment in industrial application demands the use of light structural materials for several reasons including lower gas emissions, better fuel economy and reduced energy consumption. Furthermore, taking into consideration several proprieties, Aluminum alloy is the favourable material for crafting many components for aerospace and automotive applications due to its strong corrosion resistance, low density, excellent formability and high weight to stiffness ratio.

The study was to establish the mechanical, physical and chemical properties of alloys of Aluminum. This would be used to identify the best alloy for the aerospace and automobile industries. The literature review was done sufficiently and highlighted that Aluminum alloys have become the most used metals in the automobile and aerospace manufacturing industries in the world. The alloys are used in aerospace and automobile industries because of its physical properties and durability. From the literature, it was established that important properties that make Aluminum metal useful in various manufacturing plants include its low density, excellent formability property, high strength stiffness in relation to weight and good corrosion resistance.

I will attach two more literature, analyze them same way as seen in literatures above.

Chapter Summary.

This section provides some past researches and works related to corrosion; each author studied the topic from different areas including the relationship between age hardening on microstructural characteristics of Al 7075 alloy which concluded from the experiment results that annealing heat treatment had the power to do away with micro-segregation. Also, investigation on how intergranular corrosion could be used to reduce corrosion where the authors recommend that while making any aluminum allows it was crucial to give attention to the cooling rate. Moreover, another author discussed the impact of sodium chloride, polyethylene glycol and boron on aluminum allow. In addition, another review shows that a combination of Aluminum and zinc leads to a very strong alloy. As well as the classification of aluminum alloy were studied, and the author concluded that the classification is based on temperatures used to heat and cool the alloys. This is because the temperatures are a significant determinant of the strength property as well as other features. Also, barrier coating is one of the easiest and cheapest methods in preventing corrosion in aircraft components made of aluminum. It was very effective in preventing corrosion but only if proper procedures were carried out carefully. Coating, therefore, insulates, beautifies and increases the aircraft’s life expectancy. It is also easy to apply and reflects 80% of ultraviolet rays. Though it faces certain challenges, it is very effective in preventing corrosion in aluminum, an aircraft component.

CHAPTER 3 EXPERIMENTAL SETUP

3. Introduction.

This chapter includes the steps followed in order to achieve the project objectives. First, samples preparation step which involves two parts, cutting the Aluminum alloy sheet and Numbering the samples. Then, the main step which is coating the sample using three types of coating:

· Aluminum Oxide.

· Zinc.

· Underbody Rubber coating.

After the coating step, some investigations and tests were carried out such as: Hardness test using Rockwell hardness test before and after heat treatment. Also, Roughness measurements using Mitutoyo device connected to computer software. In addition to corrosion test in sea water for 192 hours followed with a Hydrochloric test for 10 minutes in order to monitor the weight loss of the samples.

3.1 Samples Preparation.

For an accurate and fast cutting of the Aluminum alloy sheet, a mechanical guillotine called Morgan Rushworth RGMS is used.

Figure 3.1 Morgen Rushworth RGMS

Figure 3.2 Aluminum alloy sheet before cutting

The following is the procedure of cutting the Aluminum Alloy sheet using Morgen Rushworth RGMS.

1. Place the Aluminum sheet on the support table as shown in Figure 3.2.

2. Switch on machine.

3. Press SET write the desired position to the display.

4. Press START, machinery moves to the desired position.

5. Cutting operation will carried out.

6. Switch off machine.

Figure 3.3 Aluminum Alloy Sample After cutting.

Then, using metal stamps and hammer the numbering step is done by applying the following procedure:

1. Place the desired number stamp on the sample.

2. Strike twice on the stamp using the hammer.

3. The number will appear on the sample.

4. Repeat the steps using different numbers for different samples.

Figure 3.4 Metallic Stamp

Figure 3.5 Hammer

Figure 3.6 Samples After Numbering

3.2 Coating Step.

In this step I used three types of coating: Al2O3 (Aluminum Oxide), Zinc and Underbody Rubber coating.

3.2.1 Aluminum Oxide Coating:

To achieve this type of coating an Aluminum Oxide powder, Aluminum paint and a brush are required. The procedure is:

1. Prepare a mixture of 25 ml of Aluminum paint with 250 g of Al2O3.

2. Place the mixture in the rotary shaker for one hour in order to mix properly.

3. Apply the Aluminum oxide mixture on the sample using a brush.

4. Put the coated sample in a place to be exposed to air for three hours in order to dry then apply an extra layer if needed.

Figure 3.7 Aluminum Oxide and Aluminum paint.

Figure 3.8 During the Painting Step.

Figure 3.9 Sample After Applying the First layer of Coating.

3.2.2 Zinc Coating:

Zinc spray provides along-lasting cathodic corrosion protection to all metal surfaces. Zinc spray is forming a fast-drying, adherent protective layer of microfine zinc flakes. Zinc flakes are forming a resistant protective layer even under extreme weather and environmental conditions.

The following is the procedure for Zinc coating:

1. Shake the can well before using.

2. Spray evenly on the samples about 20 cm distance from the surface.

3. Put the coated sample in a place to be exposed to air for three hours in order to dry.

4. Repeat the second step until the desired thickness is obtained.

Figure 3.10 Zinc Spray and the samples Before Coating.

Figure 3.11 The Samples After Zinc Coating.

3.2.3 Underbody Rubber Coating:

This type of coating is mostly used on cars to protect them from damage, rusts, and decay. It is used in rust prevention and are applied when the car is brand and new. The manufactures are using thick paints as well as sealants for the Underbody and this is made better by the addition of the Underbody coats. Underbody coating is providing a long-lasting protection from corrosion to the car’s Underbody. It also protects parts such as the internal body panels, the frame rails, and other inner cavities which are physically accessible but are more exposed to corrosion.

The following is the procedure for underbody rubber coating:

1. Shake the can well before using.

2. Spray evenly on the samples about 20 cm distance from the surface.

3. Put the coated sample in a place to be exposed to air for three hours in order to dry.

4. Repeat the second step until the desired thickness is obtained.

Figure 3.13 The Samples After Rubber Coating.

Figure 3.12 Underbody Rubber Spray.

3.3 Heat Treatment.

Heat treatment is a group of industrial as well as metalworking processes that are utilized in altering the physical, chemical, and properties of a material. Heat treatment is also used in manufacturing of many other materials.

3.3.1 Annealing.

Annealing process is carried out through heating of a sample which has been machined, undertaken through hardness testing, and metallographic to a temperature of 4700C. Soaking such samples at a temperature of 4700C for about 2 hours is then followed by cooling process using furnace.

3.3.2 Precipitation Hardening.

This procedure is performed by using a solution to treat another set of test piece of sample which has been machined, undertaken through metallographic and hardness test at 465 °C for 2 hours. This process is then followed by quenching the samples rapidly in cold water. The quenched samples then undergo precipitation hardening, a process which is also referred to as age hardening through a heating process of the samples to 120 °C for 3 hours. The final step is the cooling process using the air within the room.

3.4 Hardness Test.

Using Rockwell hardness test which is a hardness scale based on the indentation hardness of material. Rockwell test is determining the hardness through measurement of the penetration depth of an indenter under a huger load in comparison to the penetration which has been made by the minor load.

The working principle of this device as following:

1. Select the proper indenter depending on the type of the alloy to be measured, for Aluminum Alloy 1/8 ball is used.

2. Turn the device on.

3. Place the sample to be measured on top of the anvil.

4. Rotate the anvil adjustment clock wise in order to rise the anvil till it touch the surface of the sample.

5. The reading will appear on the screen, write it down and repeat the steps using different coating samples.

Figure 3.16 Rockwell Hardness.

Figure 3.17 Indenter Used for Testing.

3.5 Roughness Measurements.

Roughness is the component of the surface texture. Its quantification is based on the deviations towards the direction of the normal vector of a real surface from the one which is considered to be ideal form. In case the deviation is large, then the surface is considered to be rough whereas if the deviations are smaller, then the surface is smooth.

The following are the steps to measure the roughness of the samples:

1. This device is connected to the computer software, first turn on the computer and the device.

2. Place the sample to be measured as shown on Figure 3.17, notice the movement of the tip on the surface of the sample for about 5 seconds.

3. The surface roughness measurements will show on the computer screen.

4. Repeat the steps using different coating samples.

Figure 3.18 Roughness device (Mitutoyo) connected to computer software.

Figure 3.19 During Roughness Measurement for Zinc sample.

3.6 Corrosion Test in Seawater.

Sea water is also known as salt water and is water from the sea or ocean. Sea water is considered to be playing a key role towards increasing the rate of corrosion. Corrosion by sea water is an electrochemical process and when it comes into contact with all metals and alloys, it makes them have specific electrical potential or corrosion potential at specific pH.

The corrosion test was carried out in Seawater In this test the samples with and without coating were immersed in sea water for 192 hours and the weight was measured before and after the test.

3.7 Corrosion Test in Hydrochloric Acid (HCl).

In this test, a solution of 100ml of HCl and 900ml of H2O was prepared and the samples with and without coating were treated with the solution for 10 minutes and the weight of the sample before and after the test were measured in order to monitor the weight loss.

Figure 3.21 Apparatus used for HCL Test.

Figure 3.22 HCl Solution.

Weight loss monitoring after the tests using digital balance in (g):

Figure 3.23 Sample Without Coating Initial Weight.

Figure 3.24 Sample Without Coating Weight After Seawater and HCL Tests.

Figure 3.25 Zinc Sample Initial Weight.

Figure 3.26 Zinc Sample Weight After Seawater and HCL Tests.

CHAPTER SUMMARY.

This chapter involves the steps followed in order to achieve the project objectives, starting with sample preparation, where an accurate cutting of Aluminum Alloy Sheet using a mechanical guillotine known as the Morgan Rushworth RGMS is performed. The metal stamps and hammer are used by placing the desired number of stamps on the sample; striking on the stamp using on hammer twice; repeating the same procedure through using different numbers for different samples, this step is important to identify the samples after coating. The next step is coating through the use of three types of coating such as Aluminum Oxide, Zinc, and the Underbody Rubber Coating. Heat treatment process is carried out through annealing, and precipitation hardening. Hardness test is performed through the use of Rockwell hardness test before and after heat treatment; followed by Roughness measurement using Mitutoyo device connected to computer software; corrosion test in sea water for 192 hours; and the last step is involving corrosion test in Hydrochloric Acid (HCL) for 10 minutes.

CHAPTER 4 RESULTS AND DISCUSSIONS

4. Introduction.

The result of this study is presented based on the outcome revealed from the tests carried out. The tests performed were related to coating processes and they included coating such as Aluminum Oxide, Zinc, and the Underbody Rubber Coating. Also, other tests included heat treatment through annealing, and precipitation hardening. Before modern metalworking techniques were invented, blacksmiths used heat to make metal workable.

Result is also collected from the hardness, Roughness measurement; corrosion test in sea water; and corrosion test in Hydrochloric Acid (HCL). Based on the outcome of these procedures, there were variations in the masses of the samples after performing the tests.

After this process the metal was quickly cooled. This process made the metal harder and less brittle. Modern metalworking has now become more sophisticated and precise, allowing for different techniques to be used for different purpose.

Keeping metals to extreme heat causes it to expand more than its initial impacting structure. Since almost everybody knows what thermal expansion is self-explanatory, I will not spend much time on it. Ductility can also be the ability to stretch metal into a wire or something similar to it.

The more the electron scatter, this symbolizes that metals have gotten hotter.

Heat treatment is a process of heating and later cooling metals. This is normally done to change their micro structure and in turn they bring out physical and mechanical characteristics that makes it more attractive. Thesss rate at which they are cooled can significantly change their metallic properties. As it can be seen that the common reason why theses undergo there is to improve their quality in terms of strength, hardness, toughness, ductility and corrosion resistance.

It was observed that different heat treatment processes gave different hardness value and impact property to the steel. The specimen with the highest hardness was found in samples quenched in water. 

They are various types of heat treatment we have annealing and precipitation hardening. In annealing it is known softens the metal, ensuring that it is more workable and providing for greater ductility. It is known as a form of metal heating bringing it closer to equilibrium state. In this particular process, the metal is heated above its upper critical temperature to change its microstructure. After that process is slowly cooled.

We have another type of heat type of heat treatment which is similar to annealing but less expensive than annealing, it s known as quenching. It concepts lies with the quick return to room temperature after it is heated above its upper critical temperature it has a vantage that it can be done by water or any form of oil.

Another method is known as precipitation hardening. It is known of creating uniformity in metal’s grain structure, making material stronger. This involves heating a metal to high temperatures after a fast cooling process. It is usually executed in an inert atmosphere at temperatures of above 900 degrees Fahrenheit. The time in which the metal is cooled and greatly depends on the length and size of the metal. This process reduces brittleness and gives out a more ductile and stable structure. We have stress relieving that is known to decrease stress in metals this is done by heating the metal to lower temperature than the required one. The metal is then slowly cooled. Normalizing is a form of heat treatment that eliminates impurities on the other hand it achieves strength and hardness. This is done by cooling the metal by air after it has been heated to a precise temperature.

When a metal is cryogenically treated, it is slowly cooled with liquid nitrogen. The slowly cooling process helps prevent thermal stress of the metal. This process helps to lower the amount of brittleness that may be caused when martensite forms during cryogenic treatment. Since the components are very expensive to produce a non-destructive hardness test is a good way to control their quality. The Vicker-method is considered to be the hardest . it uses a diamond indenter. The indenter is pressed to the surface. When it is unloaded with two diagonals between the corners. Since the load is f and average distance is d the equation for hardness will go like this.

1,8544 / ( d F H ).

4.1 Hardness Test (Before and After Heat Treatment).

Type of Coating

Reading (g)

Aluminum Oxide

129.6

Zinc

130

Underbody Rubber

129.8

Without coating

129.5

Table 4.1 Hardness Readings Before Heat Treatment.

Type of Coating

Reading (g)

Aluminum Oxide

132.1

Zinc

139.8

Underbody Rubber

135.2

Without coating

129.6

Table 4.2 Hardness Readings After Heat Treatment.

Figure 4.1 Hardness Readings Before Heat Treatment.

Figure 4.2 Hardness Readings After Heat Treatment.

First of all, you should mention that hardness after heat treatment as shown in figure 4.2 increased!!!! Why???????????? Explain the reasons in general. Why heat treatment increases the hardness of the alloys?????

4.2 Roughness Measurements.

Type of coating

Rz (µm)

Rq (µm)

Zinc

7.06

1.32

Aluminum Oxide

8.44

2.70

Underbody Rubber

11.18

1.44

Without coating

1.81

0.35

Table 4.3 Roughness Measurements.

Figure 4.3 Zinc Sample Roughness Profile.

Figure 4.4 Underbody Rubber Sample Roughness Profile.

Figure 4.5 Aluminum Oxide Sample Roughness Profile.

Figure 4.6 Without Coating Sample Roughness Profile.

Figure 4.7 Rz and Rq values of the Samples.

The relationship between roughness and corrosion goes as follows. The lower the number of roughness, the more the corrosion resistance. Surface roughness most of the time is a great influence to the corrosion, nucleation of metastable pitting and pitting potential as well. This has been confirmed by comparing all the samples before corrosion resistance tests. Here different samples created through different methods.

4.3 Weight Loss.

This step involves two parts, sea water for 192 hours followed by hydrochloric solution for about 10 minutes. The following table shows the weight loss of each coating type.

Type of Coating

Initial weight (g)

Weight after the test (g)

Weight loss

(g)

Zinc

17.588

17.534

0.054

Aluminum Oxide

17.451

17.388

0.063

Underbody Rubber

18.514

18.487

0.027

Without Coating

17.187

16.583

0.604

Table 4.4 Weight Loss.

Figure 4.8 Weight Loss (g) of the Samples.

For zinc
 
The weight loss from this treatment of zinc was attributed that it occurred at higher temperatures and can be attributed to the generation of CO/CO2 gases during reduction reactions and loss of lead in the vapour phase.
For Aluminium oxide
 
The weight loss from this treatment of Aluminium oxide was attributed that it occurred at higher temperatures of above 350 degrees and can be attributed to the generation of CO/CO2 gases during reduction reactions and loss of lead in the vapour phase.
For underbody rubber
 
The weight loss from this treatment of underbody rubber was attributed that it occurred at higher temperatures and can be attributed to the generation of CO/CO2 gases during reduction reactions and loss of lead in the vapour phase.
Without coating
 
The weight loss from this treatment of without coating was attributed that it occurred at higher temperatures and can be attributed to the generation of CO/CO2 gases during reduction reactions and loss of lead in the vapour phase.

CHAPTER SUMMARY.

This chapter involves the presentation of the outcomes in terms of the observed changes in weight and roughness measurement in micrometer (µm) from the coating processes. The results presented are based on the outcome from hardness, roughness measurement, corrosion tests in seawater, and hydrochloric acid. The Hardness readings of masses of Aluminum Oxide, Zinc, and Underbody Rubber were higher after heat treatment as compared to masses before heat. Zinc gained a lot in terms of weight after heat treatment. The outcome of the results following the immersing process of the samples with or without coating in seawater for 8 days shows that there was a minimal change. Overall results from the heat treatment show that there was an overall increase in masses of hardness following the heat treatment. The value of Zinc was the highest. The weight loss without coating was the highest with 0.604 g whereas the loss of weight in Zinc was the minimal followed by Underbody Rubber, Aluminum Oxide, and Zinc with the lowest weight loss in the procedure involving the immersing process in sea water and hydrochloric acid. Underbody rubber recorded the highest score in terms of surface roughness measurement.

It has been observed that the coated samples weight loss was less comparing with the without coated sample.

The main purpose of the heat treatment of metals and alloys is to get desired mechanical properties in term of hardness, ductility and also roughness. In this case different phases results in the different ductility, hardness and roughness. In this project, we can see how alloys cooling rates can affect micro structure and how microstructure of a specimen affects the hardness.

The Hardness readings of masses of Aluminum Oxide, Zinc, and Underbody Rubber were higher after heat treatment as compared to masses before heat treatment i.e. 132.1 g, 139.8 g, and 135.2 g, as compared to 129.6 g, 130 g, 129.8 g respectively. Zinc gained a lot in terms of weight after heat treatment. The outcome of the results following the immersing process of the samples with and without coating in seawater for 192 hours shows that there was a minimal change, followed by hydrochloric solution for 10 minutes, the weight loss without coating was the highest with 0.604 g whereas the loss of weight in Zinc was the minimal followed by Underbody Rubber, Aluminum Oxide, and Zinc with the lowest weight loss. With regard to the surface roughness, Underbody rubber recorded the highest score followed by Aluminum Oxide, Zinc, and, and without coating having the least value of surface roughness measurement.

CHAPTER 7 CONCLUSIONS

Aluminum plays an important role in a number of industrial applications such as construction and electrical engineering. Although aluminum and its alloys are quite useful, they are subject to corrosion as a result of chemical interaction with the surroundings and hence do not the best materials for engineering applications. Pitting corrosion is the main corrosion phenomenon which is common it is caused by the breakage in the oxide film. This experiment was done for the purpose of performing an experimental study on the corrosion analysis of Aluminum Alloy material used in aircraft component in order to achieve the objectives of the project by implement the corrosion resistance process experimentally and analyzing the results obtained.

The results presented are based on the outcome from hardness before and after heat treatment, roughness measurement, corrosion tests in seawater and hydrochloric acid. An overall increase in values of hardness after the heat treatment step, where Zinc coating has the highest value in terms of hardness. Also, Underbody rubber recorded the highest score in terms of surface roughness measurement.

CHAPTER 8 RECOMMENDATIONS/FUTURE WORK

In the future, it is important to have a clear understanding as well as carry out successful process of analyzing the behavior of corrosion. It is important to design Aluminum alloy when used in Aircraft so that it cannot be eroded as a result of the influencing factors such as salt, moisture, and oxygen. Coating of Aluminum alloy when used in the Aircraft should be one which is helping in the reduction of pitting corrosion which always overcomes the oxide film which is used for the protection of Aluminum alloy from corrosion. Researching and testing of the metals being used in designing the planes should be based on selecting effective ways of control the main issue i.e. pitting corrosion so that safety of public can be improved.

There are some suggestions regarding corrosion analysis of Aluminum alloy to be carried out for further future works:

· Perform the tests using different type of coating for example: Polyamide, Chrome or Titanium.

· Do the analysis using optical microscopy which gives a clear image on the corrosion initiation areas on the sample as well as the degree of deterioration of the coating used.

· Extend the period of seawater test.

REFERENCE

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6. Publicapps.caa.co.uk, 2017. Corrosion and Inspection of General Aviation Aircraft. [Online] Available at: https://publicapps.caa.co.uk/docs/33/CAP1570_Corrosion.pdf [Accessed: 8 December 2018].

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8. Top of Form

9. Wolfson Heat Treatment Centre. (1983). Guidelines for safety in heat treatment. Birmingham, Eng: Wolfson Heat Treatment Centre.

10. Bottom of Form

11. Engineering Industry Training Board. (1970). Heat treatment. Watford: Engineering Industry Training Board.

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13. Salman, J., Alsada, S. & Al-Sultani, K., 2013. Improvement Properties of 7075-T6 Aluminum Alloy by Quenching in 30% Polyethylene Glycol and Addition 0.1%B‖, Research Journal of Material Sciences, 15(4), pp.32-42.

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15. Crawford, B.R., Loader, C., Liu, Q., Harrison, T.J. and Sharp, P.K., 2014. Can pitting corrosion change the location of fatigue failures in aircraft?. International Journal of Fatigue61, pp.304-314.

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21. machining using design of experiments and neural networks. Iranian Journal of Science & Technology,

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APPENDIX I

Use extra appendixes or sections as per your requirements, the appendix may contain data, formula sheet, programmes, and extra diagrams which is required for the work and etc. as applicable for the work.

TURNITIN REPORT

Provide the first page of the Turnitin report

TECHNICAL PROJECT PROPOSAL

Provide the revised / approved TP proposal

Hardness Readings Before Heat Treatment.

Reading (g) Aluminum Oxide Zinc Underbody Rubber Without coating 132.1 139.80000000000001 135.19999999999999 129.6

Hardness Test After Heat Treatment

Reading (g) Aluminum Oxide Zinc Und erbody Rubber Without coating 132.1 139.80000000000001 135.19999999999999 129.6

RProfile

5.0000000000000001E-4 1E-3 1.5E-3 2E-3 2.5000000000000001E-3 3.0000000000000001E-3 3.5000000000000001E-3 4.0000000000000001E-3 4.4999999999999997E-3 5.0000000000000001E-3 5.4999999999999997E-3 6.0000000000000001E-3 6.4999999999999997E-3 7.0000000000000001E-3 7.4999999999999997E-3 8.0000000000000002E-3 8.5000000000000006E-3 8.9999999999999993E-3 9.4999999999999998E-3 0.01 1.0500000000000001E-2 1.0999999999999999E-2 1.15E-2 1.2E-2 1.2500000000000001E-2 1.2999999999999999E-2 1.35E-2 1.4E-2 1.4500000000000001E-2 1.4999999999999999E-2 1.55E-2 1.6E-2 1.6500000000000001E-2 1.7000000000000001E-2 1.7500000000000002E-2 1.7999999999999999E-2 1.8499999999999999E-2 1.9E-2 1.95E-2 0.02 2.0500000000000001E-2 2.1000000000000001E-2 2.1499999999999998E-2 2.1999999999999999E-2 2.2499999999999999E-2 2.3E-2 2.35E-2 2.4E-2 2.4500000000000001E-2 2.5000000000000001E-2 2.5499999999999998E-2 2.5999999999999999E-2 2.6499999999999999E-2 2.7E-2 2.75E-2 2.8000000000000001E-2 2.8500000000000001E-2 2.9000000000000001E-2 2.9499999999999998E-2 0.03 3.0499999999999999E-2 3.1E-2 3.15E-2 3.2000000000000001E-2 3.2500000000000001E-2 3.3000000000000002E-2 3.3500000000000002E-2 3.4000000000000002E-2 3.4500000000000003E-2 3.5000000000000003E-2 3.5499999999999997E-2 3.5999999999999997E-2 3.6499999999999998E-2 3.6999999999999998E-2 3.7499999999999999E-2 3.7999999999999999E-2 3.85E-2 3.9E-2 3.95E-2 0.04 4.0500000000000001E-2 4.1000000000000002E-2 4.1500000000000002E-2 4.2000000000000003E-2 4.2500000000000003E-2 4.2999999999999997E-2 4.3499999999999997E-2 4.3999999999999997E-2 4.4499999999999998E-2 4.4999999999999998E-2 4.5499999999999999E-2 4.5999999999999999E-2 4.65E-2 4.7E-2 4.7500000000000001E-2 4.8000000000000001E-2 4.8500000000000001E-2 4.9000000000000002E-2 4.9500000000000002E-2 0.05 5.0500000000000003E-2 5.0999999999999997E-2 5.1499999999999997E-2 5.1999999999999998E-2 5.2499999999999998E-2 5.2999999999999999E-2 5.3499999999999999E-2 5.3999999999999999E-2 5.45E-2 5.5E-2 5.5500000000000001E-2 5.6000000000000001E-2 5.6500000000000002E-2 5.7000000000000002E-2 5.7500000000000002E-2 5.8000000000000003E-2 5.8500000000000003E-2 5.8999999999999997E-2 5.9499999999999997E-2 0.06 6.0499999999999998E-2 6.0999999999999999E-2 6.1499999999999999E-2 6.2E -2 6.25E-2 6.3E-2 6.3500000000000001E-2 6.4000000000000001E-2 6.4500000000000002E-2 6.5000000000000002E-2 6.5500000000000003E-2 6.6000000000000003E-2 6.6500000000000004E-2 6.7000000000000004E-2 6.7500000000000004E-2 6.8000000000000005E-2 6.8500000000000005E-2 6.9000000000000006E-2 6.9500000000000006E-2 7.0000000000000007E-2 7.0499999999999993E-2 7.0999999999999994E-2 7.1499999999999994E-2 7.1999999999999995E-2 7.2499999999999995E-2 7.2999999999999995E-2 7.3499999999999996E-2 7.3999999999999996E-2 7.4499999999999997E-2 7.4999999999999997E-2 7.5499999999999998E-2 7.5999999999999998E-2 7.6499999999999999E-2 7.6999999999999999E-2 7.7499999999999999E-2 7.8E-2 7.85E-2 7.9000000000000001E-2 7.9500000000000001E-2 0.08 8.0500000000000002E-2 8.1000000000000003E-2 8.1500000000000003E-2 8.2000000000000003E-2 8.2500000000000004E-2 8.3000000000000004E-2 8.3500000000000005E-2 8.4000000000000005E-2 8.4500000000000006E-2 8.5000000000000006E-2 8.5500000000000007E-2 8.5999999999999993E-2 8.6499999999999994E-2 8.6999999999999994E-2 8.7499999999999994E-2 8.7999999999999995E-2 8.8499999999999995E-2 8.8999999999999996E-2 8.9499999999999996E-2 0.09 9.0499999999999997E-2 9.0999999999999998E-2 9.1499999999999998E-2 9.1999999999999998E-2 9.2499999999999999E-2 9.2999999999999999E-2 9.35E-2 9.4E-2 9.4500000000000001E-2 9.5000000000000001E-2 9.5500000000000002E-2 9.6000000000000002E-2 9.6500000000000002E-2 9.7000000000000003E-2 9.7500000000000003E-2 9.8000000000000004E-2 9.8500000000000004E-2 9.9000000000000005E-2 9.9500000000000005E-2 0.1 0.1005000000000000 1 0.10100000000000001 0.10150000000000001 0.10199999999999999 0.10249999999999999 0.10299999999999999 0.10349999999999999 0.104 0.1045 0.105 0.1055 0.106 0.1065 0.107 0.1075 0.108 0.1085 0.109 0.1095 0.11 0.1105 0.111 0.1115 0.112 0.1125 0.113 0.1135 0.114 0.1145 0.115 0.11550000000000001 0.11600000000000001 0.11650000000000001 0.11700000000000001 0.11749999999999999 0.11799999999999999 0.11849999999999999 0.11899999999999999 0.1195 0.12 0.1205 0.121 0.1215 0.122 0.1225 0.123 0.1235 0.124 0.1245 0.125 0.1255 0.126 0.1265 0.127 0.1275 0.128 0.1285 0.129 0.1295 0.13 0.1305 0.13100000000000001 0.13150000000000001 0.13200000000000001 0.13250000000000001 0.13300000000000001 0.13350000000000001 0.13400000000000001 0.13450000000000001 0.13500000000000001 0.13550000000000001 0.13600000000000001 0.13650000000000001 0.13700000000000001 0.13750000000000001 0.13800000000000001 0.13850000000000001 0.13900000000000001 0.13950000000000001 0.14000000000000001 0.14050000000000001 0.14099999999999999 0.14149999999999999 0.14199999999999999 0.14249999999999999 0.14299999999999999 0.14349999999999999 0.14399999999999999 0.14449999999999999 0.14499999999999999 0.14549999999999999 0.14599999999999999 0.14649999999999999 0.14699999999999999 0.14749999999999999 0.14799999999999999 0.14849999999999999 0.14899999999999999 0.14949999999999999 0.15 0.15049999999999999 0.151 0.1515 0.152 0.1525 0.153 0.1535 0.154 0.1545 0.155 0.1555 0.156 0.1565 0.157 0.1575 0.158 0.1585 0.159 0.1595 0.16 0.1605 0.161 0.1615 0.16200000000000001 0.16250000000000001 0.16300000000000001 0.16350000000000001 0.16400000000000001 0.16450000000000001 0.16500000000000001 0.16550000000000001 0.16600000000000001 0.16650000000000001 0.16700000000000001 0.16750000000000001 0.16800000000000001 0.16850000000000001 0.16900000000000001 0.16950000000000001 0.17 0.17050000000000001 0.17100000000000001 0.17150000000000001 0.17199999999999999 0.17249999999999999 0.17299999999999999 0.17349999999999999 0.17399999999999999 0.17449999999999999 0.17499999999999999 0.17549999999999999 0.17599999999999999 0.17649999999999999 0.17699999999999999 0.17749999999999999 0.17799999999999999 0.17849999999999999 0.17899999999999999 0.17949999999999999 0.18 0.18049999999999999 0.18099999999999999 0.18149999999999999 0.182 0.1825 0.183 0.1835 0.184 0.1845 0.185 0.1855 0.186 0.1865 0.187 0.1875 0.188 0.1885 0.189 0.1895 0.19 0.1905 0.191 0.1915 0.192 0.1925 0.193 0.19350000000000001 0.19400000000000001 0.19450000000000001 0.19500000000000001 0.19550000000000001 0.19600000000000001 0.19650000000000001 0.19700000000000001 0.19750000000000001 0.19800000000000001 0.19850000000000001 0.19900000000000001 0.19950000000000001 0.2 0.20050000000000001 0.20100000000000001 0.20150000000000001 0.20200000000000001 0.20250000000000001 0.20300000000000001 0.20349999999999999 0.20399999999999999 0.20449999999999999 0.20499999999999999 0.20549999999999999 0.20599999999999999 0.20649999999999999 0.20699999999999999 0.20749999999999999 0.20799999999999999 0.20849999999999999 0.20899999999999999 0.20949999999999999 0.21 0.21049999999999999 0.21099999999999999 0.21149999999999999 0.21199999999999999 0.21249999999999999 0.21299999999999999 0.2135 0.214 0.2145 0.215 0.2155 0.216 0.2165 0.217 0.2175 0.218 0.2185 0.219 0.2195 0.22 0.2205 0.221 0.2215 0.222 0.2225 0.223 0.2235 0.224 0.22450000000000001 0.22500000000000001 0.22550000000000001 0.22600000000000001 0.22650000000000001 0.22700000000000001 0.22750000000000001 0.22800000000000001 0.22850000000000001 0.22900000000000001 0.22950000000000001 0.23 0.23050000000000001 0.23100000000000001 0.23150000000000001 0.23200000000000001 0.23250000000000001 0.23300000000000001 0.23350000000000001 0.23400000000000001 0.23449999999999999 0.23499999999999999 0.23549999999999999 0.23599999999999999 0.23649999999999999 0.23699999999999999 0.23749999999999999 0.23799999999999999 0.23849999999999999 0.23899999999999999 0.23949999999999999 0.24 0.24049999999999999 0.24099999999999999 0.24149999999999999 0.24199999999999999 0.24249999999999999 0.24299999999999999 0.24349999999999999 0.24399999999999999 0.2445 0.245 0.2455 0.246 0.2465 0.247 0.2475 0.248 0.2485 0.249 0.2495 0.25 0.2505 0.251 0.2515 0.252 0.2525 0.253 0.2535 0.254 0.2545 0.255 0.2555 0.25600000000000001 0.25650000000000001 0.25700000000000001 0.25750000000000001 0.25800000000000001 0.25850000000000001 0.25900000000000001 0.25950000000000001 0.26 0.26050000000000001 0.26100000000000001 0.26150000000000001 0.26200000000000001 0.26250000000000001 0.26300000000000001 0.26350000000000001 0.26400000000000001 0.26450000000000001 0.26500000000000001 0.26550000000000001 0.26600000000000001 0.26650000000000001 0.26700000000000002 0.26750000000000002 0.26800000000000002 0.26850000000000002 0.26900000000000002 0.26950000000000002 0.27 0.27050000000000002 0.27100000000000002 0.27150000000000002 0.27200000000000002 0.27250000000000002 0.27300000000000002 0.27350000000000002 0.27400000000000002 0.27450000000000002 0.27500000000000002 0.27550000000000002 0.27600000000000002 0.27650000000000002 0.27700000000000002 0.27750000000000002 0.27800000000000002 0.27850000000000003 0.27900000000000003 0.27950000000000003 0.28000000000000003 0.28050000000000003 0.28100000000000003 0.28149999999999997 0.28199999999999997 0.28249999999999997 0.28299999999999997 0.28349999999999997 0.28399999999999997 0.28449999999999998 0.28499999999999998 0.28549999999999998 0.28599999999999998 0.28649999999999998 0.28699999999999998 0.28749999999999998 0.28799999999999998 0.28849999999999998 0.28899999999999998 0.28949999999999998 0.28999999999999998 0.29049999999999998 0.29099999999999998 0.29149999999999998 0.29199999999999998 0.29249999999999998 0.29299999999999998 0.29349999999999998 0.29399999999999998 0.29449999999999998 0.29499999999999998 0.29549999999999998 0.29599999999999999 0.29649999999999999 0.29699999999999999 0.29749999999999999 0.29799999999999999 0.29849999999999999 0.29899999999999999 0.29949999999999999 0.3 0.30049999999999999 0.30099999999999999 0.30149999999999999 0.30199999999999999 0.30249999999999999 0.30299999999999999 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[mm]

[um]

RProfile

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[mm]

[um]

RProfile

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1.35 1.3 1.25 1.27 1.28 1.31 1.32 1.44 1.47 1.47 1.46 1.45

[mm]

[um]

RProfile

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[mm]

[um]

Surface Roughness Measurments

Rz (µm) Zinc Aluminum Oxide Underbody Rubber Without coating 7.06 8.44 11.18 1.81 Rq (µm) Zinc Aluminum Oxide Underbody Rubber Without coating 1.32 2.7 1.44 0.35

Type of coating

Measurment of surface roughness Rz and Rq

Weight Loss (g)

Weight loss (g) Zinc Aluminum Oxide Underbody Rubber Without Coating 5.3999999999999999E-2 6.3E-2 2.7E-2 0.60399999999999998