Spectroscopy
Joedavid437 
Question6-ChinconaAlkaloid-inDMSO-d6.pdf.pdf
1.52.02.53.03.54.04.55.05.56.06.57.07.58.08.59.0 f1 (ppm)
3. 21
1. 11
1. 05
1. 03
3. 04
2. 16
2. 13
1. 07
1. 05
0. 98
1. 11
1. 09
1. 08
0. 99
1. 07
1. 00
1. 43
1. 45
1. 47
1. 49
1. 70
1. 85
1. 87
1. 89
2. 18
2. 19
2. 55
2. 56
2. 63
2. 65
2. 67
2. 95
2. 96
2. 97
2. 98
2. 99
3. 01
3. 02
3. 03
5. 06
5. 08
5. 11
5. 29
5. 30
5. 69
5. 69
6. 06
6. 07
6. 08
6. 09
6. 10
6. 11
6. 12
7. 54
7. 55
7. 59
7. 61
7. 62
7. 72
7. 73
7. 74
8. 01
8. 03
8. 25
8. 26
8. 83
8. 84
7.57.67.78.08.18.28.38.88.9 f1 (ppm)
45 25
.0 45
29 .4
45 57
.5 45
64 .6
45 72
.6
46 31
.9 46
39 .1
46 47
.0
48 09
.4 48
17 .7
49 51
.1 49
59 .5
53 02
.6 53
06 .9
5.05.15.25.35.76.16.2 f1 (ppm)
30 36
.4 30
47 .6
30 66
.5
31 77
.5 31
82 .8
34 12
.5 34
16 .7
36 38
.3 36
46 .0
36 48
.4 36
55 .9
36 63
.1 36
65 .5
36 73
.3
1.51.71.92.62.93.1 f1 (ppm)
1. 00
A (s) 1.70
85 8.
3 87
2. 9
88 2.
5 89
1. 6
10 18
.6
11 11
.4 11
21 .4
11 32
.8
13 05
.8 13
13 .8
15 27
.7 15
37 .8
15 89
.6 16
00 .1
17 77
.5 17
81 .6
18 04
.7 18
12 .8
DMSO-d6
HOD
Question 6, 1H
-100102030405060708090100110120130140150160170180190200210 f1 (ppm)
24 .4
26 .7
28 .2
48 .7
49 .5
61 .3
71 .4
11 4.
9 11
9. 5
12 4.
7 12
6. 5
12 6.
7 12
9. 2
13 0.
1
14 1.
7
14 8.
3 15
0. 5
15 1.
3
Question 6, 13C
1.21.41.61.82.02.22.42.62.83.05.05.25.45.65.86.07.67.88.08.28.48.68.89.0 f2 (ppm)
1.5
2.0
2.5
3.0
5.0
5.5
6.0
7.5
8.0
8.5
9.0
f1 (
pp m
)
Question 6, gCOSY
1.52.02.53.05.05.56.07.58.08.59.0 f2 (ppm)
1.5
2.0
2.5
3.0
3.5 5.0
5.5
6.0
7.5
8.0
8.5
9.0
f1 (
pp m
)
Question 6, gNOESY
1.52.02.53.03.54.04.55.05.56.06.57.07.58.08.59.0 f2 (ppm)
30
40
50
60
70
80
90
100
110
120
130
140
150
f1 (
pp m
)
Question 6, HSQC
1.52.02.53.03.54.04.55.05.56.07.58.08.59.0 f2 (ppm)
30
40
50
60
70
120
130
140
150
f1 (
pp m
)
Question 6, gHMBC
